====== Fabricating SNSPDs ====== Fabrication based on Nb(Ti)N ===== Film deposition ===== ^ Group ^ Year ^ Publication ^ Process ^ Recipe ^ Notes ^ | Karl K. Berggren et al. \\ **NbN** | 2009 | {[Dauler:2009]} | DC magnetron sputtering | Sapphire, 800C, 8 mTorr, with 100 sccm Ar, 5 sccm N2 | Parameters varied: deposition time, substrate material and deposition pressure. \\ Deposition time strongly influences the yield. (Pg 60,61) | | ::: | 2015 | {[Najafi.Dane.ea:2015]} | DC magnetron sputtering | as above | Solvent cleaning exposure to an oxygen plasma (20% 02 in He) 100 W for 3 min | | ::: | 2017 | {[Zhu:2017]} | DC magnetron sputtering | AlN, 840C, Ar, N2 26.5sccm, 8sccm, 2.5mTorr | Sheet resistance goal between 500-530 Ohm/sq | | Jeff F. Young \\ **NbTiN** | 2017 | {[Yan:2017]} | DC magnetron sputtering | STAR Cryoelectronics Inc. Commercial | | | Robert Hadfield \\ **NbTiN** | <2017 | {[Kirkwood:2017} | DC magnetron sputtering | STAR Cryoelectronics Inc. Commercial | | | ::: | 2017 | {[Banerjee:2017]} | DC magnetron sputtering | Own developed | | ===== Lithography ===== ^ Group ^ Year ^ Publication ^ Resist ^ Recipe ^ Notes ^ | Karl K. Berggren et al. \\ **NbN** | -- | -- | -- | -- | | Jeff F. Young . \\ **NbTiN** | 2017 | {[Yan:2017]} |ZEP520A (past shelf life) (Positive resist) (markers) | 500nm, 180C 3 min, o-xylene | Preparation: DI water, 2min US, Acetone, 2min US, IPA, 2min US. N2 dry, 100C dehydration for 1 min| | ::: | ::: | ::: | (negative resist)(meander) | 150nm, 180C 3 min | ::: | | Wolfram Pernice . \\ **NbN** | 2018 | {[Munzberg.Vetter.ea:2018]} | HSQ | | Cover the NbN with a SiO2 layer to protect against oxidation and as adhesion promoter for HSQ.| ===== Pattern transfer ===== All of the groups in literature use a dry etching process to transfer the pattern on the film. ^ Group ^ Year ^ Publication ^ Process Gases ^ Recipe ^ Notes ^ | Karl K. Berggren \\ **NbN** | <2015 | {[Dauler:2009]}, {[Yang:2005]} | CF4 | 10mTorr, 15sccm CF4, 100W RF power | | | ::: | 2015 | {[Najafi.Mower.ea:2015]}, {[Najafi.Dane.ea:2015]}, {[Najafi:2015]} | CF4| 50W | rest of recipe not mentioned. | | ::: | 2017 | {[Zhu:2017]} | CF4, He| 10mTorr, He, CF4, 7sccm, 15sccm, 50W | Cleaning etch before with CF4 and O2. Over-etching reduces device yield. | | Jeff F. Young \\ **NbTiN** | 2017 | {[Yan:2017]} | CF4, O2 | 30mTorr, 15sccm CF4, 2 sccm O2, 50W RF power | No saturating results seen. | | Robert Hadfield \\ **NbTiN** | 2017 | {[Kirkwood:2017]} | CF4 | 30mTorr, 50sccm CF4, 80W RF power | Not sure about the quality of the detectors | | Wolfram Pernice . \\ **NbN** | 2018 | {[Munzberg.Vetter.ea:2018]} | Fluorine based | | Cover the NbN with a SiO2 layer to protect against oxidation and as adhesion promoter for HSQ.| ===== Characterization ===== The different techniques for Film characterization given by different groups. ^ Group ^ Method ^ Publication ^ Notes ^ | Karl K. Berggren \\ **NbN** | $R_\mathrm{RT} / R_\mathrm{20K} $ | {[Zhu:2017]} | Comparing the value at RT vs just above Transition temperature allows to investigate impurities. Good Films had on the order of 0.84 | | ::: | $\Delta T_C$ | {[Zhu:2017]} | Difference between the temperature of 10% of $R_\mathrm{20K}$ and 90% of $R_\mathrm{20K}$. Good Films had approx 1.8K| | ::: | $T_C$ | {[Zhu:2017]} | Resistance below $50\% ~ R_\mathrm{20K}$|