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topic:optics:quantumoptics:detection:sspd:process

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Fabricating SNSPDs

Fabrication based on Nb(Ti)N

Film deposition

Group Year Publication Process Recipe Notes
Karl K. Berggren et al.
NbN
2009 \cite{Dauler:2009} DC magnetron sputtering Sapphire, 800C, 8 mTorr, with 100 sccm Ar, 5 sccm N2 Parameters varied: deposition time, substrate material and deposition pressure.
Deposition time strongly influences the yield. (Pg 60,61)
2015 \cite{Najafi.Dane.ea:2015} DC magnetron sputtering as above Solvent cleaning exposure to an oxygen plasma (20% 02 in He) 100 W for 3 min
2017 \cite{Zhu:2017} DC magnetron sputtering AlN, 840C, Ar, N2 26.5sccm, 8sccm, 2.5mTorr Sheet resistance goal between 500-530 Ohm/sq
Jeff F. Young
NbTiN
2017 \cite{Yan:2017} DC magnetron sputtering STAR Cryoelectronics Inc. Commercial
Robert Hadfield
NbTiN
<2017 \cite{Kirkwood:2017} DC magnetron sputtering STAR Cryoelectronics Inc. Commercial
2017 \cite{Banerjee:2017} DC magnetron sputtering Own developed

Lithography

Group Year Publication Resist Recipe Notes
Karl K. Berggren et al.
NbN
Jeff F. Young .
NbTiN
2017 \cite{Yan:2017} ZEP520A (past shelf life) (Positive resist) (markers) 500nm, 180C 3 min, o-xylene Preparation: DI water, 2min US, Acetone, 2min US, IPA, 2min US. N2 dry, 100C dehydration for 1 min
(negative resist)(meander) 150nm, 180C 3 min
Wolfram Pernice .
NbN
2018 \cite{Munzberg.Vetter.ea:2018} HSQ Cover the NbN with a SiO2 layer to protect against oxidation and as adhesion promoter for HSQ.

Pattern transfer

All of the groups in literature use a dry etching process to transfer the pattern on the film.

Group Year Publication Process Gases Recipe Notes
Karl K. Berggren
NbN
<2015 \cite{Dauler:2009}, \cite{Yang:2005} CF4 10mTorr, 15sccm CF4, 100W RF power
2015 \cite{Najafi.Mower.ea:2015}, \cite{Najafi.Dane.ea:2015}, \cite{Najafi:2015} CF4 50W rest of recipe not mentioned.
2017 \cite{Zhu:2017} CF4, He 10mTorr, He, CF4, 7sccm, 15sccm, 50W Cleaning etch before with CF4 and O2. Over-etching reduces device yield.
Jeff F. Young
NbTiN
2017 \cite{Yan:2017} CF4, O2 30mTorr, 15sccm CF4, 2 sccm O2, 50W RF power No saturating results seen.
Robert Hadfield
NbTiN
2017 \cite{Kirkwood:2017} CF4 30mTorr, 50sccm CF4, 80W RF power Not sure about the quality of the detectors
Wolfram Pernice .
NbN
2018 \cite{Munzberg.Vetter.ea:2018} Fluorine based Cover the NbN with a SiO2 layer to protect against oxidation and as adhesion promoter for HSQ.

Characterization

The different techniques for Film characterization given by different groups.

Group Method Publication Notes
Karl K. Berggren
NbN
$R_\mathrm{RT} / R_\mathrm{20K} $ \cite{Zhu:2017} Comparing the value at RT vs just above Transition temperature allows to investigate impurities. Good Films had on the order of 0.84
$\Delta T_C$ \cite{Zhu:2017} Difference between the temperature of 10% of $R_\mathrm{20K}$ and 90% of $R_\mathrm{20K}$. Good Films had approx 1.8K
$T_C$ \cite{Zhu:2017} Resistance below $50\% ~ R_\mathrm{20K}$
topic/optics/quantumoptics/detection/sspd/process.1616780352.txt.gz · Last modified: by samuel